2-Cyano-N′-[(E)-1-(2-oxo-2H-chromen-3-yl)ethylidene]acetohydrazide

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2-Cyano-N′-[(E)-1-(2-oxo-2H-chromen-3-yl)ethyl­idene]acetohydrazide

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The phenyl ring in title mol-ecule, C(16)H(11)NO(3), forms a dihedral angle of 7.69 (6)° with the fused ring system. The observed conformation is stabilized by intra-molecular N-H⋯O and C-H⋯O inter-actions. In the crystal, supra-molecular chains are formed along the b axis which are mediated by π-π inter-actions [centroid-centroid distance = 3.614 (2) Å].

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There are two independent mol-ecules in the asymmetric unit of the title compound, C16H15NO3S2, in which the pyrrolidine rings adopt envelope conformations, with a methyl-ene C atom as the flap. The dihedral angles betweeen the near-planar 2H-chromene ring systems [maximum deviations = 0.0167 (20) and 0.0136 (19) Å] and the pyrrolidine rings (all atoms) are 83.83 (11) and 82.43 (11)°. In the cr...

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The title compound, C(12)H(10)BrN(3)O(2)S, exists in an E configuration with respect to the C=N bond. The approximately planar 2H-chromene ring system [maximum deviation = 0.059 (1) Å] is inclined at a dihedral angle of 17.50 (5)° with respect to the mean plane through the thio-semicarbazide unit and an intra-molecular N-H⋯N hydrogen bond generates an S(5) ring. In the crystal structure, adjace...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2012

ISSN: 1600-5368

DOI: 10.1107/s1600536812019915